{"id":2,"date":"2017-04-27T11:03:30","date_gmt":"2017-04-27T11:03:30","guid":{"rendered":"https:\/\/www.staff.ncl.ac.uk\/michaelprobert\/?page_id=2"},"modified":"2018-04-12T10:34:55","modified_gmt":"2018-04-12T10:34:55","slug":"equipment","status":"publish","type":"page","link":"https:\/\/www.staff.ncl.ac.uk\/michaelprobert\/equipment\/","title":{"rendered":"Diffraction Equipment"},"content":{"rendered":"

\"20180412_095335\"<\/p>\n

Bruker D8 Vantage – Cu and Ag microfocus X-ray sources and a Photon II detector on a 3 circle fixed chi goniometer. This diffractometer is fitted with\u00a0an\u00a0Oxford Cryosystems n-Helix and Cryostream 800.<\/p>\n

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\"20180412_095604\"<\/p>\n

XIPHOS I: a custom\u00a0built bespoke diffractometer for the study of crystalline samples at ultra low temperatures. The system couples a Huber 4-circle goniometer with a Bruker TXS Mo rotating anode X-ray source and an APEX II CCD detector. Cooling to a base temperature of 1.86 K is achieved through a modified 3 stage APD 202E closed cycle cryocooler.\u00a0https:\/\/doi.org\/10.1107\/S0021889810041282<\/a><\/p>\n

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\"20180412_095712\"<\/p>\n

XIPHOS II: another custom built instrument specialising in the measurement of single crystal samples at very high pressures, provided through the use of diamond anvil cells. The system couples a 4 circle Huber goniometer, a Ag microfocus X-ray source and an APEXII CCD detector.<\/p>\n

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\"20180412_095626\"<\/p>\n

An Oxford Diffraction (now Rigaku Oxford Diffraction) Gemini Ultra with Cu and Mo sealed tube X-ray sources. This system operates with an Oxford Cryosystems Cryostream 700 to maintain temperatures in the 400-90 K range. This is the departmental workhorse for service crystallographic studies.<\/p>\n

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\"20180412_095831\"<\/p>\n

A Bruker D2 Phaser powder diffractometer, used predominantly for analysis of bulk samples to check the consistency of phase purity.<\/p>\n","protected":false},"excerpt":{"rendered":"

Bruker D8 Vantage – Cu and Ag microfocus X-ray sources and a Photon II detector on a 3 circle fixed chi goniometer. This diffractometer is fitted with\u00a0an\u00a0Oxford Cryosystems n-Helix and Cryostream 800. XIPHOS I: a custom\u00a0built bespoke diffractometer for the … Continue reading →<\/span><\/a><\/p>\n","protected":false},"author":1238,"featured_media":0,"parent":0,"menu_order":0,"comment_status":"closed","ping_status":"open","template":"","meta":{"footnotes":""},"class_list":["post-2","page","type-page","status-publish","hentry"],"_links":{"self":[{"href":"https:\/\/www.staff.ncl.ac.uk\/michaelprobert\/wp-json\/wp\/v2\/pages\/2","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/www.staff.ncl.ac.uk\/michaelprobert\/wp-json\/wp\/v2\/pages"}],"about":[{"href":"https:\/\/www.staff.ncl.ac.uk\/michaelprobert\/wp-json\/wp\/v2\/types\/page"}],"author":[{"embeddable":true,"href":"https:\/\/www.staff.ncl.ac.uk\/michaelprobert\/wp-json\/wp\/v2\/users\/1238"}],"replies":[{"embeddable":true,"href":"https:\/\/www.staff.ncl.ac.uk\/michaelprobert\/wp-json\/wp\/v2\/comments?post=2"}],"version-history":[{"count":5,"href":"https:\/\/www.staff.ncl.ac.uk\/michaelprobert\/wp-json\/wp\/v2\/pages\/2\/revisions"}],"predecessor-version":[{"id":42,"href":"https:\/\/www.staff.ncl.ac.uk\/michaelprobert\/wp-json\/wp\/v2\/pages\/2\/revisions\/42"}],"wp:attachment":[{"href":"https:\/\/www.staff.ncl.ac.uk\/michaelprobert\/wp-json\/wp\/v2\/media?parent=2"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}